|
Sample Preparation: Power-Prep™ System
DESCRIPTION
|
Power-Prep™ System
The Power-Prep™ is a high speed sample processing work station. It
is designed to automate the extraction and cleanup of
toxic compounds such as Dioxins, PCBs, Pesticides, and
PAHs from environmental, biological and food samples.
Power-Prep processes from 1 to 10 samples in less than 1 hour,
thereby,achieving high recoveries and excellent precision for all
target compounds.
The Power-Prep™ system fits into the smallest budget. With its modular design, you can cost effectively
automate your extraction and sample clean-up procedures by purchasing a 1-sample system and expand it to 5 or 10
samples as needed.
|
|
|
FEATURES
|
- Real-time plotting of UV, pH, Conductivity, and Temperature.
- Purification parameters can be changed during the run.
- Ability to save UV, pH, Conductivity and Temperature data every 0.5
second.
- Programmable flow rate ranges 0.02ml ~ 1000ml/min.
- Saved data can be reviewed and compressed.
- Method development tool.
- Runs from small scale to production scale purification.
|
PRINCIPLES OF OPERATION |
Power-Prep™ is changing the face of high speed sample processing
in today's laboratories. The computer controlled liquid chromatography
system performs simultaneous sample processing automatically and
unattended. You need only to load your samples, snap on your pre-packed
columns and press the start key. The system performs
the entire extraction and cleanup automatically including
sample loading, washing, elution and fraction collection.
The Power-Prep™ system separates Dioxins, PCBs, and Pesticides
for 5 samples in less than one hour.
Software
FMS’s powerful windows- based monitoring and control software offers a rich set of features and flexibility.
It includes functions to develop and optimize methods. Input parameters include flow rates, volumes, column selection,
sample size, solvent selection and fraction collection.
Hardware
Each Power-Prep™ system contains multiple quick connect modules consisting of:
- Power Supply Module
- Control Module
- Pump & Pressure Modules
- Valve Drive Modules
- Sample Processing Modules
The Power-Prep modules are mounted vertically on a portable cabinet. It is a self contained system that
also provides storage for solvent bottles, waste and collectors.
Modular and Expandable
A one sample PowerPrep system can be expanded up to a 10 sample configuration. Both expansion and
module replacement are done via FMS’s quick connect modules. This feature reduces system down time and
increases laboratory throughput.
Applications
Sample Clean-Up
The Power-Prep sample clean-up system separates Dioxins, PCBs, and Pesticides from a variety of
sample extracts such as:
- Soils
- Water
- Fly Ash
- Milk
- Air
- Waste
- Human Serum
- Adipose Tissue
- Fish Samples
- Waste Water
- Pulp & Paper
Solid Phase Extraction (SPE)
In addition to sample clean-up the Power-Prep automates the entire Solid Phase Extraction of Dioxins,
PCBs and Pesticides from a variety of aqueous samples such as:
- Water
- Milk
- Waste Water
- Human Serum
Saves Time & Money
With a few keystrokes, the Power-Prep system performs an entire column chromatography, automatically
achieving high recoveries for all analytes. The unattended operation feature of the system saves labor and valuable time.
The Power-Prep system reduces the amount of glassware and solvents required for manual sample clean-up.
Uses Disposable Columns
The Power-Prep System uses pre packed disposable columns. FMS’s proprietary columns are made from teflon and
contain multi layer silica, alumina, and carbon. FMS’s prepacked columns are tested for purity and performance
prior to shipment.
Yields High Recoveries
The combination of FMS’s patented pump controller and patented prepacked disposable teflon columns produces
high recoveries for all analytes.
The following are typical recoveries using a spiked sample:
- 2378 - TCDD ................................. 75
- 2378 - TCDF .................................. 70
- 12378 - PeCDD .............................. 80
- 12378 - PeCDF .............................. 80
- 23478 - PeCDF ............................... 84
- 123478 - HXCDD ........................... 91
- 123678 - HXCDD ........................... 78
- 123789 - HXCDD ........................... 87
- 123478 - HXCDF ........................... 86
- 123678 - HXCDF ........................... 85
- 123789 - HXCDF ........................... 90
- 234678 - HXCDF ........................... 82
- 1234678 - HpCDF .......................... 82
- 1234678 - HXCDF .......................... 89
- OCDD ............................................. 74
- OCDF ............................................. 74
- 3344 - PCB (PCB 77) ..................... 78
- 3445 - PCB (PCB81) ...................... 82
- 33445 - PCB (PCB 126) ................. 85
- 334455 - PCB (PCB169) ................ 77
System Configuration
Power-Prep™/p (Parallel)
Parallel sample clean-up System for Dioxins, PCBs and Pesticides sample analysis.
Capacity: 1 to 10 samples
Processing time: 1 hour per run
Columns:
- Multi-layer Silica
- Alumina
- Carbon
Column Material: Teflon
Power-Prep™/s (Sequential)
Sequential sample clean-up System for Dioxins, PCBs and Pesticides sample analysis.
Capacity: 5 samples
Processing time: 5 hours per run
Columns:
- Multi-layer Silica
- Alumina
- Carbon
Column Material: Teflon
Power-Prep™/SPE
Automated Solid Phase Extraction System for automating EPA, SW-846
methods for pesticides, PCBs and PAHs sample analysis.
Capacity: 5 to 25 samples
Processing time: 1 to 5 hours per run
Columns:
- Silica
- Alumina
- Carbon
- Florisil
- C18
Column Material: Teflon, Polypropylene
Power-Prep™/GPC
Automated GPC Clean-up System for automating EPA, SW-846 GPC Clean-up method for pesticides, PCBs and PAHs
sample analysis.
Capacity: 5 to 25 samples
Processing time: 5 to 25 hours per run
Packing Material: Styrene-DiVinylBenzene
Column Material: Teflon, Glass
|
|
© 2003 Fluid Management Systems. All Rights Reserved.
Webmaster
|
|